TY - JOUR PY - 1983// TI - Analysis of the major metabolite of delta 9-tetrahydrocannabinol in urine II. A HPLC procedure JO - Journal of analytical toxicology A1 - Wells, K. E. A1 - Dimson, P. A. A1 - Jones, A. B. A1 - ElSohly, H. N. A1 - ElSohly, M. A. SP - 262 EP - 264 VL - 7 IS - 6 N2 - A high performance liquid chromatographic (HPLC) procedure was developed for the analysis of 11-nor-delta 9-tetrahydrocannabinol-9-carboxylic acid in urine. Hydrolyzed urine samples were cleaned up using Bond-Elut columns. 11-Nor-cannabinol-9-carboxylic acid was used as internal standard. The analysis was carried out using a C8 reversed-phase column with acetonitrile:50 mM phosphoric acid (65:35) as the solvent. Detection was done by ultraviolet detector at 214 nm. The minimum detectable level of 11-nor-delta 9-tetrahydrocannabinol-9-carboxylic acid was 25 ng/mL.

Language: en

LA - en SN - 0146-4760 UR - http://dx.doi.org/ ID - ref1 ER -