TY - JOUR PY - 1997// TI - The confirmation of volatiles by solid-phase microextraction and GC-MS in the investigation of two traffic fatalities JO - Journal of analytical toxicology A1 - Brewer, W. E. A1 - Galipo, R. C. A1 - Morgan, S. L. A1 - Habben, K. H. SP - 286 EP - 290 VL - 21 IS - 4 N2 - A simple, sensitive, and reliable method was developed for the confirmation of nonroutine volatiles in the investigation of two traffic fatalities. Solid-phase microextraction (SPME) fibers were used to extract volatile compounds from the headspace of sample vials; components were subsequently analyzed by gas chromatography-mass spectrometry (GC-MS). In the first case, ethanol and methylene chloride were detected in a urine sample by headspace SPME and GC-MS. The second case involved the analysis of volatile petroleum products from submitted specimens by headspace SPME and GC-MS. In both cases, SPME and GC-MS analyses provided crucial evidence in the investigation of the traffic fatalities.
Language: en
LA - en SN - 0146-4760 UR - http://dx.doi.org/ ID - ref1 ER -